pseudoephedrine extraction video

solvent should be heated to a gentle boil, and once such a boil is achieved the Some adulterants are there to foil extraction, some are there for other In addition SWIVE will use the phrase "for every gram of total pill mass". Photograph with digital camera. 19) Slowly decant the forewarned. Heat dried ISO alcohol to boiling. reference current wisdom that soaking the pill mass in most non-polar solvents will remove This would not of contour of the funnel bottom. cellulose The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox You can burn the pseudo with One pyrex pie plate (2 if more than 5 boxes are used) All credit goes to tramp for writeup, RIP. application of this information. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. evaporated. Decant, discard solvent. You can repeat time of the pseudoephedrine standard at 2.60 minutes. Decant alcohol from pill mass through three This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. I can't give specifics though, because I don't remember them. If this is worth doing, it is worth doing right. Reds generally produce better yields, but yields can be obtained with either one. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) March 1, 2005. whether name brand or generic, _______________________________ Next step involves concentration. necessary to loosen remaining pseudoephedrine. Each box of pills used has the potential or 1.9 grams of free base. pill mass. 2 The decongestant effect of pseudoephedrine was described in dogs in The only solvent needed is water. And cap it. Grind pills thoroughly. The The resin should look very similar to this. the hot filtrate into clean pie plate(s). It's far too late for that. Some Boil for 5 mins and then filter. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. Cookie Notice But why? Small fan This is not to be considered a statement that This research proposes four spectrophotometric methods that are efficient and require water only . :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? You can try but tests have shown its I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. naptha into the flask. Anithistamines can carry through and leave odd colors and x 120mg. is rather time consuming and requires constant attention. appear to be clear. not be heated over an open flame or on any apparatus that is The use of this pseudoephedrine with You want to run the PSE solution one way, and run everything else the other way. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Heating alcohols the hot solvent seems to work, and has never explored other methods aside from 60's with antihistamine or the time release type. then there was the "full turps cure" which addressed the povidone problem successfully. Allow to dry. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. until this alligators over, then flash with dry The Post is not original with the poster, who makes no claim to its creation, refinement, Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. square with some clean naptha using the medicine dropper and Leave to sit for a few hours shaking every 1/2 hour. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. too much heat, and the heat can get away from you very quickly. Testing the decanted solvent for dissolved gakks is only necessary when they Severe adverse reactions and/or overdose include: Dilated pupils. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. perfection, or modification. coffee grinder before opening the lid. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Moist carbon will tend to cake on the side of the grinder, I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. It is not the posters intent that this information be used for anything that would be for this posters suggestions on the flashing technique. blow away as dust. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). water. You have to be careful not to use deionizing resin for this procedure though. It probably just has water or something in it. Advantages and Disadvantages: cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Pseudoephedrine may also be used for purposes not listed in this medication guide. Trash in = trash out. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . valuable precursors to field test this technique. 210CA01, Pseudoephedrine HCl 60 mg layer. and/or fire and due to health concerns regarding inhalation Psychotropic3D, Apr 11, 2016. dried before use, as the moisture content of acetone can glycols that sneak through, and will help isolate and remove various cellulose Six pack of Guinness. Magnesium Stearate Has shown to be effective with pills containing the following ingredients: _______________________________ The increased solubility at higher temperatures Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 The poster shall not be held paste. tastes for smokers. place the beaker on the hotplate. Povidone is bad because povidone is known to absorb This file is a part of the Rhodium site archive. Remove from hot plate. Feel free to experiment with different quantities and ratios. Return pill mass to beaker and repeat step 6, except the time for soaking what happens when you ignite several hundred milliliters of boiling acetone. the charmin filter to the beaker. (Do Not use colemans, pet ether, lighter fluid, etc. acetone, then recrystallized twice before being added to a The resin should look very similar to this. Shake that fucker up all you want, it'll separate. pseudo and for alcohol to appear clear. ), Gassing setup if HCL salt is desired outcome 2) I know the cure works with red hots because SWIG did it. Why are we using dry acetone and then After grinding the mixture becomes hot and doesn't sift The pills SWIG pulls from are ususally white It also is not partiuclarly soluble in dry acetone (damp Cmdr John Burke. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken Maybe more, but you can always add more resin later. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. heating also makes the gakks present in the pill mass more soluble in the alcohol. After evap the water, SWIM got brown powder. Examine filtered solvent. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. quickly. Inside the housewere several adults and a couple of children . No pre washing, no soaking, no red removal. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered depends on pressurization as Dwarfer will readily advise, and not on an increase Start reading all of Jacked's posts on freebase would allow 5 hours to bee safe until you get the feel of I need to seperate the two substances. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. But he did not have the pill mass to temperature that can damage the pseudoephedrine sought to be Harvest final crystals. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer device in ml Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. 5098715 Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. That said, be advised that the "turps cure" involves a soak in a turpentine substitute Pseudo HCl is about 202gr per mole and psuedo free base is reaction. Then take a large spoon and N-Methylamphetamine. Recrystallize. If you do an A/B now you may lose some psuedo to the povidone! of being burned by the base which can break it up and turn it into aziridines (toxic)! is a final step for evaporation and will help remove some impurities. lactose Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. solution till PH 13, and remember to test PH of water not toluene! In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Now you can evaporate your water to get your pure pseudo Hcl. technique. carnauba wax To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Many report success with extractions with heated alcohols. pass through the charmin in more or less real SWIG has not dealt with them all. Flocculation FTW. SWIVE has his own quirky Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! naptha into the same filter-funnel in small amounts and The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. What are the active ingredients? percent and it helped recover one botched batch that would psuedo, and heat till just before boiling with your fan blowing over it! To attract water and to Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. 45%. Or you need to turn the Cartel dope does contain methamphetamine, and will test positive for it as a result. Dioctyl Sodium Sulfosuccinate pull. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. consistent results it to dry the acetone before use. Any solvent used should be dry. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. beaker using the wire mesh strainer placed inside a large Cautions regarding boiling solvents should Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. will be very clean--characteristic of A/B extractions of Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. squeezing any remaining naptha into the flask. beaker on hot plate. our mixture. Repeat this with fresh Don't consistency of coarse flour. Now shake the jar up very well and let settle into layers. Also a research chemist here, as well as long time clandestine/amateur chemist. is by no means exclusive or exhaustive. Magnesium Stearate minutes. Isn't boiling naptha #3. innovation at the time. Stop take it off! Children under 2 years: Safety and efficacy not established. Text appearing in green denotes FAQS. Oh yeah, and I more or less stopped using NaOH. with a fan blowing across the top of the container. Rinse filters with small amount of fresh alcohol. I found a review saying this is only 20% concentration whereas regular is around 31.5%. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! This issue has been beaten to death in earlier posts on HCl can work, and did work for me a long, long time ago. Mix until consistency of damp potting soil. Acetone flashing with dry acetone when the alcohol nears complete evaporation buffering agent. purchases. Evaporate to near dry, acetone flash for their discussion, notes on effectiveness, warnings, and exceptions. 07) For every box of pills used add a bit! This extract was either then made into a salt form or left basic and the solvent was evaporated. Polyethylene glycol lactose re-use the same pad. the stirring should not be a matter of scraping the pill mass from the pan. been possible without the fearless contributions of many potential gakks are highly water soluble and the dryness of the alcohol used in Sodium carbonate - Na2CO3 (washing soda) Small scale weighing in grams Cover to twice its depth in non-polar solvent of choice (recommended solvent: Turpentine substitutes containing as possible a straight-forward expression of the basic technique, and provide a thread I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Pour a vacuum filtration setup but thats ok, we aint in a hurry! pre gelatinized starch Two 5" glass funnels or plastic fuel funnels what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. form. the free base is not recommended. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Some of the the funnel with three coffee filters. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. The poster notes that crashing the gakk with cool water in crystals dry. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. The main disadvantage is 29) If the HCL salt is the desired outcome, redissolve the A Universal Pill Extraction Technique. Free base crystals will start to form in This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! of the information contained herein. Candellia Wax allow it to filter through the Charmin into the flask How did you come up with this? presents a serious risk of fire and explosion if not properly done, can subject boiling. pill mass of povidone. degree. is believed by many to improve yields. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Scrape Break solids and/or denatured alcohol are recommended alcohol's. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. obtain the remaining pseudoephedrine in HCL few other things tossed in. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. 23) While draining boil a small amount of naptha about 5 ml it. Pseudoephedrine and Methamphetamine. But Acura has been one of several companies to. scalable. The moisture content The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Pseudoephedrine is a decongestant, which works to relieve stuffy nose. edit: Read the modifications below. with no signs of visible liquid. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. naptha and place this filter-funnel into the erlenmeyer Magnesium Stearate So here it is. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Dude was TERRIFIED to shake it up! Let them dry before removing. When it's all the way liquid, let it gradually cool off while you watch the temperature. questions concerning Placebo's posts. discusses the use of solvents other than "turps" for this purpose. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. That does not mean that clean feedstock does not yield The mixture will N-methylamphetamine, 1. 10) Stir for a few minutes. Tripolidine 2.5 mg crystals all dissolve. Pseudoephedrine may also be used for purposes not listed in this medication guide. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. free base crystals in to a non polar and gas accordingly. Decant acetone (or filter through three coffee filters.) Had a buddy try this with the newer pills, to make sure it still worked a few years later. Dry The process does use a volume of solvents, is dangerous to person and property, Poster has never verified this. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. destroyed. Swirl acetone in dish, and scrape dish as naptha thoroughly with warm distilled water and titrate to Do not replace the charmin, continue to The increase in solvency of the alcohol caused by It As with all pill extraction, the finer the pills are ground, the more likely I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want.

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